A staple for any lab, the IA30 Fourier Transform Infrared (FTIR) Spectrometer is a high-performance benchtop instrument.

A staple for any lab, the IA30 Fourier Transform Infrared (FTIR) Spectrometer is a high-performance benchtop instrument.

The IA30 is the perfect choice for analytical and research applications such as polymer, semiconductor, and pharmaceutical samples, offering simple operation as well as fast and accurate results. IR absorption, transmission, reflectance, and infrared photoluminescence can all be measured in the IA30 using only one software package, Miracle™.

The IA30 is a modern benchtop FTIR instrument with guaranteed hardware and software performance. A robust interferometer is at the core of the IA30 and is built on an anti-vibration frame to minimize any influence from the environment. The interferometer features a solid-state reference laser with a long operating life. The combination of a stable, high-intensity IR source and broadband DLaTGS detector ensures repeatability and accuracy, resulting in a robust and reliable instrument producing data that you can trust.

Features:

Outstanding Performance: High sensitivity and spectral resolution
User-friendly: Simple to operate and suitable for all user levels, from beginner to advanced
Maintenance Free: No maintenance required with moisture control technology
Customizable: Range of accessories for different sample types and measurements.
Miracle™ Software: Powerful and intuitive software designed specifically for the IA30

High spectral resolution from 0.5 cm-1 is available for measurements of narrow infrared lines, up to a resolution of 32 cm-1 for recording of fast kinetic processes.

All IA30 specifications are guaranteed, and every individual instrument goes through rigorous validation procedures to ensure that your spectrometer meets the high standards of Edinburgh Analytical.

MEASUREMENT EXAMPLES

ATR-FTIR

ATR-FTIR is the dominant FTIR method for analysis of solids and liquids as it requires little to no sample preparation and is non-destructive. With ATR-FTIR an Internal Reflective Element (IRE) is used as the ATR crystal that the beam of radiation is directed into. 

ATR-FTIR spectrum of Human serum.

Figure 1: ATR-FTIR spectrum of Human serum.

A range of materials are available for the ATR crystal, and the decision of which one to pick is based on application area. ZnSe is suitable for routine analysis, however, harder samples can cause the crystal to crack or shatter and strongly acidic or basic samples can cause toxic fumes. Germanium is suited to samples with a high refractive index and surface studies due to its smaller depth of penetration. The gold standard material for ATR crystals is diamond; it’s virtually indestructible, whilst offering high thermal conductivity for heated ATR-FTIR experiments. 

Transmission FTIR spectroscopy is the most traditional method to analyse samples. Incident infrared light passes through the sample, and the amount which transmits through is measured producing an FTIR spectrum in %Transmission. 

FTIR spectrum of CO2 gas

Figure 1: FTIR spectrum of CO2 gas 

Transmission FTIR can be used for liquids, solids, and essential for gas phase measurements. Sample preparation is typically required for transmission measurements; solid samples may require dispersion in KBr and pressed into pellets, and IR transparent windows, such as CaF2, are required for measuring liquids.  

The IA30 can host numerous other sampling accessories, offering a full suite of FTIR techniques. For example, specular reflectance accessories are particularly useful for analysing thin films. Diffuse reflectance infrared Fourier transform spectroscopy (DRIFTS) is excellent for collecting IR spectra from strongly absorbing samples with rough surfaces, such as powders.  

Temperature study on a water-in-oil emulsion

Figure 1: Temperature study on a water-in-oil emulsion  

Accessories are designed for specific end user needs, for example heated ATRs can be offered to track phase transitions in samples. Liquid transmission cells are offered to allow for fast and easy application of the sample, and for cleaning between samples with huge benefits to sample throughput. 

FTIR spectrum of ethanol with a 50 μm path length

Figure 2: FTIR spectrum of ethanol with a 50 μm path length

Specifications

Standard ConfigurationSpectral Range8000 – 350 cm-¹
SensitivitySNR ≥ 20,000:1
Resolution0.5 cm-¹, 1 cm-¹, 2 cm-¹, 4 cm-¹, 8 cm-¹, 16 cm-¹, 32 cm-¹
Accuracy0.5 cm-¹
SourceHigh-intensity ceramic source
DetectorDLaTGS
BeamsplitterGermanium coated KBr
Hygroscopic IntegrityIntegrated desiccants, electronic dry-membrane, embedded LCD and software hygrometers for maintenance-free operation
WindowsKBr window exchangeable by user
Operating VoltageUniversal mains input 100-240 VAC, 47-63 Hz
Sample AccessoriesTransmission Sample HolderCompatible with films and cuvettes
Attenuated Total Reflectance (ATR)Basic and advanced ATR models available with a choice of crystal (diamond, Ge, ZnSe)
OthersDiffuse reflectance, custom and third-party accessories available
SoftwareMiraclePC-controlled software
Measurement TypesTransmission, Absorption, Reflection, Kubelka-Munk
Acquisition ModesLive signal monitoring, single scan (including user-defined methods), kinetic series
DimensionsW x D x H660 mm x 540 mm x 300 mm
Weight37 kg

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IA30
FTIR Spectrometer
IA30
FTIR Spectrometer